Practical Organic Chemistry

Amita Dua | Amita Malik | Category: Chemistry

Binding Type: Paperback Binding

Book DetailsISBN: 9789384370428
YOP: 2017
Pages: 264Order also on

The book has been written to provide assistance to the undergraduate students of various Universities. The Organic Practicals have been written taking care of the green route to synthesis in organic chemistry and minimum use of chemicals. The book covers the synthesis of organic derivatives of compounds with different functional groups. Methodology have been given in detail for carrying out systematic functional group analysis and estimation of functional group analysis. The book covers basic principles of crystallisation, application and importance of melting/boiling point determination in detail. Chromatographic separation by different
chromatographic techniques involving paper, thin layer and column are described. Isolation of active components from different sources and identification of organic compounds by IR and NMR techniques have been covered. The book is very comprehensive covering all aspects from calculations for preparation of reagents to observations and writing of results. “Practicals made easy” is the slogan of the book. Efforts have been put in to simplify each step to help in solving difficulties generally faced during experimentation. This would thus provide an in-depth understanding to the students with the habit of scientific reasoning.

EXPERIMENT 1: RECRYSTALLISATION
EXPERIMENT 2: MELTING POINT
EXPERIMENT 3: BOILING POINT
EXPERIMENT 4: CHROMATOGRAPHY
I. Paper Chromatography
II. Thin Layer Chromatography
III. Column Chromatography
EXPERIMENT 5: FUNCTIONAL GROUP ANALYSIS OF ORGANIC COMPOUNDS
EXPERIMENT 6: OXIDATION
EXPERIMENT 7: REDUCTION
EXPERIMENT 8 : HYDROLYSIS
EXPERIMENT 9: ADDITION
EXPERIMENT 10: HALOGENATION
EXPERIMENT 11: NITRATION
EXPERIMENT 12: ACYLATION
I. Acetylation
II. Benzoylation

The book has been written to provide assistance to the undergraduate students of various Universities. The Organic Practicals have been written taking care of the green route to synthesis in organic chemistry and minimum use of chemicals. The book covers the synthesis of organic derivatives of compounds with different functional groups. Methodology have been given in detail for carrying out systematic functional group analysis and estimation of functional group analysis. The book covers basic principles of crystallisation, application and importance of melting/boiling point determination in detail. Chromatographic separation by different
chromatographic techniques involving paper, thin layer and column are described. Isolation of active components from different sources and identification of organic compounds by IR and NMR techniques have been covered. The book is very comprehensive covering all aspects from calculations for preparation of reagents to observations and writing of results. “Practicals made easy” is the slogan of the book. Efforts have been put in to simplify each step to help in solving difficulties generally faced during experimentation. This would thus provide an in-depth understanding to the students with the habit of scientific reasoning.

EXPERIMENT 1: RECRYSTALLISATION
EXPERIMENT 2: MELTING POINT
EXPERIMENT 3: BOILING POINT
EXPERIMENT 4: CHROMATOGRAPHY
I. Paper Chromatography
II. Thin Layer Chromatography
III. Column Chromatography
EXPERIMENT 5: FUNCTIONAL GROUP ANALYSIS OF ORGANIC COMPOUNDS
EXPERIMENT 6: OXIDATION
EXPERIMENT 7: REDUCTION
EXPERIMENT 8 : HYDROLYSIS
EXPERIMENT 9: ADDITION
EXPERIMENT 10: HALOGENATION
EXPERIMENT 11: NITRATION
EXPERIMENT 12: ACYLATION
I. Acetylation
II. Benzoylation